From: Influence of the amino-terminal sequence on the structure and function of HIV integrase
Data collection | Overall (highest shell) |
---|---|
Space group | P43211 |
Unit cell dimensions | 102.919 Å × 102.919 Å × 279.203 Å; 90°, 90°, 90° |
Resolution range (Å) | 96.567–2.40 |
Rmerge | 0.558 (1.619) |
Rp.i.m. | 0.110 (0.318) |
CC1/2 | 0.990 (0.289) |
Multiplicity | 26.6 (26.6) |
I/σ | 8.1 (1.6) |
Completeness (%) | 100 (100) |
Refinement | |
 Reflections (work) | 58,492 |
 Reflections (free) | 1169 |
 Rwork | 22.5% |
 Rfree | 25.3% |
 Protein atoms | 12,003 |
 Ligand/ion atoms | 28 |
 Water molecules | 226 |
 R.m.s. bonds (Å) | 0.004 |
 R.m.s. angles (°) | 0.589 |
 Ramachandran plot (%) | |
  Favored | 98.49 |
  Allowed | 1.51 |
  Outliers | 0.00 |